Dynamic Recrystallization Behavior During Thermal Deformation of Ti-43Al-0.5Re-xCr Alloy
Author of the article: SHAOQihang1, CHU Yudong1,2, CHEN Xiaofei1, WEI Beibei1, MA Biao1, TANG Bin1,2
Author's Workplace:1. State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, China; 2. Sanhang Advanced Materials Research Institute Co., Ltd., Chongqing 401135, China
Key Words:TiAl alloy; thermal deformation; dynamic recrystallization; Cr content; microstructure evolution; flow curve
Abstract:
TiAl alloys, novel lightweight, high-temperature metal structural materials, feature low density, high specific
strength, and excellent high-temperature performance. However, its narrow hot working window and poor deformation at
high temperatures make the formation of alloy components difficult. Adding β-stabilizing elements enhances hot
deformation by introducing a disordered β-phase, but the mechanism is unclear. Therefore, Ti-43Al-0.5Re-xCr (x=1, 1.5, 2,
at.%) alloys were used as the research objects, and thermal mechanical compression experiments were conducted at 1 150,
1 200 and 1 250 ℃. Flow curves under different conditions were analysed, the effects of temperature and Cr content on the
thermal deformation microstructure and dynamic recrystallization were studied, and the microstructural evolution of the
Ti-43Al-0.5Re-1.5Cr alloy at 1 200 ℃/0.01 s-1 was clarified. The results indicate that the overall flow stress of the alloy
decreases with increasing deformation temperature and Cr content. When the alloys are deformed at 1 150 ℃, many
residual lamellar colonies exist in the microstructure that primarily fragment through bending, twisting, and breaking, leading to high deformation resistance. When the alloys are deformed at 1 200 or 1 250 ℃, most of the alloy microstructure
is the α phase, which undergoes continuous dynamic recrystallization, resulting in low deformation resistance. Under
deformation conditions of 1 200 ℃, a 0.01 s-1 strain rate, and 40% deformation, the degree of recrystallization in the alloy
increases with increasing β phase content. Thus, an increase in the Cr content enhances the content of the β phase in the
alloy, which promotes the dynamic recrystallization process of the alloy. In the deformed microstructure of the Ti-43Al
0.5Re-1.5Cr alloy at 1 200 ℃, a strain rate of 0.01 s-1, and 40% deformation, many low angle grain boundaries (LAGBs, 2°
~15° misorientation) are distributed around the fine β phases, which interconnect to form numerous small-sized subgrains,
resulting in the formation of fine recrystallized grains. Thus, the β phase plays a role in refining the recrystallized grains.
The microstructures of the Ti-43Al-0.5Re-1.5Cr alloy samples subjected to different strains were studied, revealing their
microstructure evolution at 1 200 ℃/0.01 s-1 hot deformation.